LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

Kumar Motiram-Corral; Alexandre A. Souza; Josep Sauri; Pau Nolis; Teodor Parella

doi:10.1002/cphc.201901142

LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

Kumar Motiram-Corral, Alexandre A. Souza, Josep Sauri, Pau Nolis, Teodor Parella

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Resumen

The optimum detection and accurate measurement of longer-range ((4)J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated C-13 and N-15 nuclei using the LR-selHSQMBC experiment.

Idioma original	Inglés
Páginas (desde-hasta)	280-283
Número de páginas	4
Publicación	ChemPhysChem
Volumen	21
N.º	4
Fecha en línea anticipada	17 ene 2020
DOI	https://doi.org/10.1002/cphc.201901142
Estado	Publicada - feb 2020
Publicado de forma externa	Sí

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abstract = "The optimum detection and accurate measurement of longer-range ((4)J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated C-13 and N-15 nuclei using the LR-selHSQMBC experiment.",

keywords = "NMR spectroscopy, Heteronuclear coupling constants, Long-range heteronuclear connectivities, Proton-deficient molecules structure elucidation, time-sharing NMR",

author = "Kumar Motiram-Corral and Souza, {Alexandre A.} and Josep Sauri and Pau Nolis and Teodor Parella",

year = "2020",

month = feb,

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AU - Sauri, Josep

AU - Nolis, Pau

AU - Parella, Teodor

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KW - NMR spectroscopy

KW - Heteronuclear coupling constants

KW - Long-range heteronuclear connectivities

KW - Proton-deficient molecules structure elucidation

KW - time-sharing NMR

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LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

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