TY - JOUR
T1 - Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate
AU - Piniella, J. F.
AU - Rius, J.
AU - Alvarez-Larena, A.
AU - Batllori, X.
AU - Victory, P.
PY - 1991/8
Y1 - 1991/8
N2 - The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) Å, β=96.03(2)°, Vc =3069 Å3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 Å. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring.
AB - The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) Å, β=96.03(2)°, Vc =3069 Å3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 Å. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring.
UR - http://www.scopus.com/inward/record.url?scp=0348033405&partnerID=8YFLogxK
U2 - 10.1007/BF01160664
DO - 10.1007/BF01160664
M3 - Article
AN - SCOPUS:0348033405
SN - 0277-8068
VL - 21
SP - 489
EP - 494
JO - Journal of Crystallographic and Spectroscopic Research
JF - Journal of Crystallographic and Spectroscopic Research
IS - 4
ER -