Efficient and fast sign-sensitive determination of heteronuclear coupling constants

Josep Saurí; Pau Nolis; Teodor Parella

doi:10.1016/j.jmr.2013.08.013

Efficient and fast sign-sensitive determination of heteronuclear coupling constants

Josep Saurí
, Pau Nolis
, Teodor Parella^*

^*Corresponding author for this work

Research output: Indexed journal article › Article › peer-review

16 Citations (Scopus)

Abstract

Two complementary 1D NMR approaches for the fast and easy determination of the magnitude and the sign of heteronuclear J(XH) coupling constants are proposed: The Up&Down technique relies on the direct analysis of anti-phase multiplets whereas the Left&Right technique is based on the relative displacement between separate IPAP components.

Original language	English
Pages (from-to)	66-69
Number of pages	4
Journal	Journal of Magnetic Resonance
Volume	236
DOIs	https://doi.org/10.1016/j.jmr.2013.08.013
Publication status	Published - 2013
Externally published	Yes

Keywords

Heteronuclear coupling constants
HSQMBC-TOCSY
IPAP
Sign of coupling constants

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10.1016/j.jmr.2013.08.013

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title = "Efficient and fast sign-sensitive determination of heteronuclear coupling constants",

abstract = "Two complementary 1D NMR approaches for the fast and easy determination of the magnitude and the sign of heteronuclear J(XH) coupling constants are proposed: The Up\&Down technique relies on the direct analysis of anti-phase multiplets whereas the Left\&Right technique is based on the relative displacement between separate IPAP components.",

keywords = "Heteronuclear coupling constants, HSQMBC-TOCSY, IPAP, Sign of coupling constants",

author = "Josep Saur{\'i} and Pau Nolis and Teodor Parella",

year = "2013",

doi = "10.1016/j.jmr.2013.08.013",

language = "English",

volume = "236",

pages = "66--69",

journal = "Journal of Magnetic Resonance",

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publisher = "Academic Press Inc.",

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TY - JOUR

T1 - Efficient and fast sign-sensitive determination of heteronuclear coupling constants

AU - Saurí, Josep

AU - Nolis, Pau

AU - Parella, Teodor

PY - 2013

Y1 - 2013

N2 - Two complementary 1D NMR approaches for the fast and easy determination of the magnitude and the sign of heteronuclear J(XH) coupling constants are proposed: The Up&Down technique relies on the direct analysis of anti-phase multiplets whereas the Left&Right technique is based on the relative displacement between separate IPAP components.

AB - Two complementary 1D NMR approaches for the fast and easy determination of the magnitude and the sign of heteronuclear J(XH) coupling constants are proposed: The Up&Down technique relies on the direct analysis of anti-phase multiplets whereas the Left&Right technique is based on the relative displacement between separate IPAP components.

KW - Heteronuclear coupling constants

KW - HSQMBC-TOCSY

KW - IPAP

KW - Sign of coupling constants

UR - https://www.scopus.com/pages/publications/84884215757

U2 - 10.1016/j.jmr.2013.08.013

DO - 10.1016/j.jmr.2013.08.013

M3 - Article

AN - SCOPUS:84884215757

SN - 1090-7807

VL - 236

SP - 66

EP - 69

JO - Journal of Magnetic Resonance

JF - Journal of Magnetic Resonance

ER -

Efficient and fast sign-sensitive determination of heteronuclear coupling constants

Abstract

Keywords

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