Structure of 7-Amino-5-bromo-4-methyl-2-oxo-l,2,3,4-tetrahydro-l,6- naphthyridine-8-carbonitrile Monohydrate

D. Gómez De AndéRez; Ano J.R. Helliwell; E. J. Dodson; J. F. Piniella; G. Germain; A. Alvarez-Larena; J. Teixido; P. Victory

doi:10.1107/S0108270191007175

Structure of 7-Amino-5-bromo-4-methyl-2-oxo-l,2,3,4-tetrahydro-l,6- naphthyridine-8-carbonitrile Monohydrate

D. Gómez De AndéRez
, Ano J.R. Helliwell^*
, E. J. Dodson
, J. F. Piniella
, G. Germain
, A. Alvarez-Larena
, J. Teixido
, P. Victory

^*Autor corresponent d’aquest treball

Producció científica: Article en revista indexada › Article › Avaluat per experts

13 Cites (Scopus)

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C₁₀H₉BrN₄0.H₂0, Mr=299.13, monoclinic, C2/c, α=21.938(2), b=16.003(1), c = 6-847 (1) Å,β = 98.32 (1) °, V= 2378.5 A 3, Z = 8, Dm = 1-71, D_x = 1.670 g cm -3, λ(Mo Kα) = 0.71069 A, = 33.57 cm-1, F(000) Å μ= 1200, room temperature, R = 0.053 for 1379 observed reflections. The X-ray diffraction study shows that the compound obtained in the cyclization of 5-cyano-6-(dicyanomethylene)-4- methyl-2-piperidone in HBr/dioxane is the title compound.

Idioma original	Anglès
Pàgines (de-a)	104-106
Nombre de pàgines	3
Revista	Acta Crystallographica Section C
Volum	48
Número	1
DOIs	https://doi.org/10.1107/S0108270191007175
Estat de la publicació	Publicada - 15 de gen. 1992

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@article{70b5dda0138944c58ecd66472eb0c7e6,

title = "Structure of 7-Amino-5-bromo-4-methyl-2-oxo-l,2,3,4-tetrahydro-l,6- naphthyridine-8-carbonitrile Monohydrate",

abstract = "C10H9BrN40.H20, Mr=299.13, monoclinic, C2/c, α=21.938(2), b=16.003(1), c = 6-847 (1) {\AA},β = 98.32 (1) °, V= 2378.5 A 3, Z = 8, Dm = 1-71, Dx = 1.670 g cm -3, λ(Mo Kα) = 0.71069 A, = 33.57 cm-1, F(000) {\AA} μ= 1200, room temperature, R = 0.053 for 1379 observed reflections. The X-ray diffraction study shows that the compound obtained in the cyclization of 5-cyano-6-(dicyanomethylene)-4- methyl-2-piperidone in HBr/dioxane is the title compound.",

author = "\{De And{\'e}Rez\}, \{D. G{\'o}mez\} and Helliwell, \{Ano J.R.\} and Dodson, \{E. J.\} and Piniella, \{J. F.\} and G. Germain and A. Alvarez-Larena and J. Teixido and P. Victory",

year = "1992",

month = jan,

day = "15",

doi = "10.1107/S0108270191007175",

language = "English",

volume = "48",

pages = "104--106",

journal = "Acta Crystallographica Section C",

issn = "0108-2701",

publisher = "International Union of Crystallography",

number = "1",

}

TY - JOUR

T1 - Structure of 7-Amino-5-bromo-4-methyl-2-oxo-l,2,3,4-tetrahydro-l,6- naphthyridine-8-carbonitrile Monohydrate

AU - De AndéRez, D. Gómez

AU - Helliwell, Ano J.R.

AU - Dodson, E. J.

AU - Piniella, J. F.

AU - Germain, G.

AU - Alvarez-Larena, A.

AU - Teixido, J.

AU - Victory, P.

PY - 1992/1/15

Y1 - 1992/1/15

N2 - C10H9BrN40.H20, Mr=299.13, monoclinic, C2/c, α=21.938(2), b=16.003(1), c = 6-847 (1) Å,β = 98.32 (1) °, V= 2378.5 A 3, Z = 8, Dm = 1-71, Dx = 1.670 g cm -3, λ(Mo Kα) = 0.71069 A, = 33.57 cm-1, F(000) Å μ= 1200, room temperature, R = 0.053 for 1379 observed reflections. The X-ray diffraction study shows that the compound obtained in the cyclization of 5-cyano-6-(dicyanomethylene)-4- methyl-2-piperidone in HBr/dioxane is the title compound.

AB - C10H9BrN40.H20, Mr=299.13, monoclinic, C2/c, α=21.938(2), b=16.003(1), c = 6-847 (1) Å,β = 98.32 (1) °, V= 2378.5 A 3, Z = 8, Dm = 1-71, Dx = 1.670 g cm -3, λ(Mo Kα) = 0.71069 A, = 33.57 cm-1, F(000) Å μ= 1200, room temperature, R = 0.053 for 1379 observed reflections. The X-ray diffraction study shows that the compound obtained in the cyclization of 5-cyano-6-(dicyanomethylene)-4- methyl-2-piperidone in HBr/dioxane is the title compound.

UR - https://www.scopus.com/pages/publications/0000817488

UR - https://www.webofscience.com/api/gateway?GWVersion=2&SrcApp=pure_univeritat_ramon_llull&SrcAuth=WosAPI&KeyUT=WOS:A1992HB16300038&DestLinkType=FullRecord&DestApp=WOS

U2 - 10.1107/S0108270191007175

DO - 10.1107/S0108270191007175

M3 - Article

AN - SCOPUS:0000817488

SN - 0108-2701

VL - 48

SP - 104

EP - 106

JO - Acta Crystallographica Section C

JF - Acta Crystallographica Section C

IS - 1

ER -

Structure of 7-Amino-5-bromo-4-methyl-2-oxo-l,2,3,4-tetrahydro-l,6- naphthyridine-8-carbonitrile Monohydrate

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