LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

Kumar Motiram-Corral; Alexandre A. Souza; Josep Sauri; Pau Nolis; Teodor Parella

doi:10.1002/cphc.201901142

LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

Kumar Motiram-Corral
, Alexandre A. Souza
, Josep Sauri
, Pau Nolis
, Teodor Parella

Producció científica: Article en revista indexada › Article › Avaluat per experts

1 Citació (Web of Science)

Resum

The optimum detection and accurate measurement of longer-range ((4)J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated C-13 and N-15 nuclei using the LR-selHSQMBC experiment.

Idioma original	Anglès
Pàgines (de-a)	280-283
Nombre de pàgines	4
Revista	ChemPhysChem
Volum	21
Número	4
Data online anticipada	17 de gen. 2020
DOIs	https://doi.org/10.1002/cphc.201901142
Estat de la publicació	Publicada - de febr. 2020
Publicat externament	Sí

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10.1002/cphc.201901142

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abstract = "The optimum detection and accurate measurement of longer-range ((4)J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated C-13 and N-15 nuclei using the LR-selHSQMBC experiment.",

keywords = "NMR spectroscopy, Heteronuclear coupling constants, Long-range heteronuclear connectivities, Proton-deficient molecules structure elucidation, time-sharing NMR",

author = "Kumar Motiram-Corral and Souza, \{Alexandre A.\} and Josep Sauri and Pau Nolis and Teodor Parella",

year = "2020",

month = feb,

doi = "10.1002/cphc.201901142",

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AU - Souza, Alexandre A.

AU - Sauri, Josep

AU - Nolis, Pau

AU - Parella, Teodor

PY - 2020/2

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AB - The optimum detection and accurate measurement of longer-range ((4)J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long-range couplings can be simultaneously determined for protonated and non-protonated C-13 and N-15 nuclei using the LR-selHSQMBC experiment.

KW - NMR spectroscopy

KW - Heteronuclear coupling constants

KW - Long-range heteronuclear connectivities

KW - Proton-deficient molecules structure elucidation

KW - time-sharing NMR

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LR-selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long-Range Heteronuclear NMR Correlations

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