Implementing multiplicity editing in selective HSQMBC experiments

Josep Saurí, Eduard Sistaré, R. Thomas Williamson, Gary E. Martin, Teodor Parella*

*Autor corresponent d’aquest treball

Producció científica: Article en revista indexadaArticleAvaluat per experts

10 Cites (Scopus)

Resum

Even C/CH2 and odd CH/CH3 carbon-multiplicity information can be directly distinguished from the relative positive/negative phase of cross-peaks in a novel ME (Multiplicity-Edited)-selHSQMBC experiment. The method can be extended by a TOCSY propagation step, and it is fully compatible for the simultaneous and precise determination of long-range heteronuclear coupling constants. Broadband homonuclear decoupling techniques can also be incorporated to enhance sensitivity and signal resolution by effective collapse of J(HH) multiplets.

Idioma originalAnglès
Pàgines (de-a)170-175
Nombre de pàgines6
RevistaJournal of Magnetic Resonance
Volum252
DOIs
Estat de la publicacióPublicada - de març 2015
Publicat externament

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