Heat flow reaction calorimetry under reflux conditions

R. Nomen; J. Sempere; P. Lerena

doi:10.1016/0040-6031(93)80193-E

Heat flow reaction calorimetry under reflux conditions

R. Nomen, J. Sempere, P. Lerena

Departament d'Enginyeria Química i Ciència de Materials

Producció científica: Article en revista indexada › Article › Avaluat per experts

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A brief review of the procedures used in heat flow reaction calorimetry experiments under reflux and their evaluation is presented. A method to calibrate global heat transfer coefficients and the mass flow of the cooling condenser fluid under refluxing conditions is validated and discussed through experiments with pure solvents. A study of the influence of the most significant experimental conditions on the accuracy of the measurements is also considered.

Idioma original	Anglès
Pàgines (de-a)	263-276
Nombre de pàgines	14
Revista	Thermochimica Acta
Volum	225
Número	2
DOIs	https://doi.org/10.1016/0040-6031(93)80193-E
Estat de la publicació	Publicada - 11 d’oct. 1993

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@article{0e21e839505a46a69206ac0c2aa81753,

title = "Heat flow reaction calorimetry under reflux conditions",

abstract = "A brief review of the procedures used in heat flow reaction calorimetry experiments under reflux and their evaluation is presented. A method to calibrate global heat transfer coefficients and the mass flow of the cooling condenser fluid under refluxing conditions is validated and discussed through experiments with pure solvents. A study of the influence of the most significant experimental conditions on the accuracy of the measurements is also considered.",

author = "R. Nomen and J. Sempere and P. Lerena",

year = "1993",

month = oct,

day = "11",

doi = "10.1016/0040-6031(93)80193-E",

language = "English",

volume = "225",

pages = "263--276",

journal = "Thermochimica Acta",

issn = "0040-6031",

publisher = "Elsevier B.V.",

number = "2",

}

TY - JOUR

T1 - Heat flow reaction calorimetry under reflux conditions

AU - Nomen, R.

AU - Sempere, J.

AU - Lerena, P.

PY - 1993/10/11

Y1 - 1993/10/11

N2 - A brief review of the procedures used in heat flow reaction calorimetry experiments under reflux and their evaluation is presented. A method to calibrate global heat transfer coefficients and the mass flow of the cooling condenser fluid under refluxing conditions is validated and discussed through experiments with pure solvents. A study of the influence of the most significant experimental conditions on the accuracy of the measurements is also considered.

AB - A brief review of the procedures used in heat flow reaction calorimetry experiments under reflux and their evaluation is presented. A method to calibrate global heat transfer coefficients and the mass flow of the cooling condenser fluid under refluxing conditions is validated and discussed through experiments with pure solvents. A study of the influence of the most significant experimental conditions on the accuracy of the measurements is also considered.

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U2 - 10.1016/0040-6031(93)80193-E

DO - 10.1016/0040-6031(93)80193-E

M3 - Article

AN - SCOPUS:0000758143

SN - 0040-6031

VL - 225

SP - 263

EP - 276

JO - Thermochimica Acta

JF - Thermochimica Acta

IS - 2

ER -

Heat flow reaction calorimetry under reflux conditions

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